Valorization of mulberry (Rubus glaucus) by-products: ultrasound-assisted extraction of total anthocyanins
In this study, the objective was to establish parameters of optimization of the factors such as solvent concentration, extraction time and liquid-to-solid ratio in ultrasound-assisted extraction (UAE) of total anthocyanins from mulberry by-products. The study sample corresponds to mature fruits that...
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2019
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I11-R107article-27082020-04-22T13:37:49Z Valorization of mulberry (Rubus glaucus) by-products: ultrasound-assisted extraction of total anthocyanins Valorization of mulberry (Rubus glaucus) by-products: ultrasound-assisted extraction of total anthocyanins Ordóñez-Santos, Luis Eduardo Esparza-Estrada, Jessica Osorio Mora, Oswaldo diseño compuesto central metodología de superficie de respuesta colorante natural optimización central composite design response surface methodology natural colorant optimization In this study, the objective was to establish parameters of optimization of the factors such as solvent concentration, extraction time and liquid-to-solid ratio in ultrasound-assisted extraction (UAE) of total anthocyanins from mulberry by-products. The study sample corresponds to mature fruits that did not comply with the size demanded by the market (by-product). Three independent variables including extraction time (6-74 min), liquid-solid ratio (33-66.16 mL/g), and ethanol concentration (63-96%) were investigated. A rotatable central composite design (CCD) and response surface methodology (RSM) was used to investigate the effect of process variables. The optimum conditions of ultrasound-assisted extraction obtained through response surface methodology were as follow: extraction time, 20 min; liquid to solid ratio, 60:1 mL/g, and ethanol concentration, 90%, allowed to obtain a maximum concentration of 259.66 mg/L. To validate the optimized model, the experimental values were compared with the predicted values to check the adequacy of the model. Ultrasound extraction was 13.60% higher than maceration technique and reduces the time from 24h to 20 minutes. The results show that ultrasonic-assisted extraction as a promising agro-industrial process in the recovery of anthocyanins from mulberry by-products. In this study, the objective was to establish parameters of optimization of the factors such as solvent concentration, extraction time and liquid-to-solid ratio in ultrasound-assisted extraction (UAE) of total anthocyanins from mulberry by-products. The study sample corresponds to mature fruits that did not comply with the size demanded by the market (by-product). Three independent variables including extraction time (6-74 min), liquid-solid ratio (33-66.16 mL/g), and ethanol concentration (63-96%) were investigated. A rotatable central composite design (CCD) and response surface methodology (RSM) was used to investigate the effect of process variables. The optimum conditions of ultrasound-assisted extraction obtained through response surface methodology were as follow: extraction time, 20 min; liquid to solid ratio, 60:1 mL/g, and ethanol concentration, 90%, allowed to obtain a maximum concentration of 259.66 mg/L. To validate the optimized model, the experimental values were compared with the predicted values to check the adequacy of the model. Ultrasound extraction was 13.60% higher than maceration technique and reduces the time from 24h to 20 minutes. The results show that ultrasonic-assisted extraction as a promising agro-industrial process in the recovery of anthocyanins from mulberry by-products. Facultad de Ciencias Agrarias-UNCuyo 2019-12-09 info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion application/pdf https://revistas.uncu.edu.ar/ojs3/index.php/RFCA/article/view/2708 Revista de la Facultad de Ciencias Agrarias UNCuyo; Vol. 51 No. 2 (2019): July-December; 367-380 Revista de la Facultad de Ciencias Agrarias UNCuyo; Vol. 51 Núm. 2 (2019): Julio-Diciembre; 367-380 1853-8665 0370-4661 eng https://revistas.uncu.edu.ar/ojs3/index.php/RFCA/article/view/2708/1967 Derechos de autor 2019 Revista de la Facultad de Ciencias Agrarias UNCuyo |
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Revistas en línea |
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Revistas en línea |
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Revista de la Facultad de Ciencias Agrarias |
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Revista de la Facultad de Ciencias Agrarias |
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eng |
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author |
Ordóñez-Santos, Luis Eduardo Esparza-Estrada, Jessica Osorio Mora, Oswaldo |
spellingShingle |
Ordóñez-Santos, Luis Eduardo Esparza-Estrada, Jessica Osorio Mora, Oswaldo Valorization of mulberry (Rubus glaucus) by-products: ultrasound-assisted extraction of total anthocyanins diseño compuesto central metodología de superficie de respuesta colorante natural optimización central composite design response surface methodology natural colorant optimization |
author_facet |
Ordóñez-Santos, Luis Eduardo Esparza-Estrada, Jessica Osorio Mora, Oswaldo |
author_sort |
Ordóñez-Santos, Luis Eduardo |
title |
Valorization of mulberry (Rubus glaucus) by-products: ultrasound-assisted extraction of total anthocyanins |
title_short |
Valorization of mulberry (Rubus glaucus) by-products: ultrasound-assisted extraction of total anthocyanins |
title_full |
Valorization of mulberry (Rubus glaucus) by-products: ultrasound-assisted extraction of total anthocyanins |
title_fullStr |
Valorization of mulberry (Rubus glaucus) by-products: ultrasound-assisted extraction of total anthocyanins |
title_full_unstemmed |
Valorization of mulberry (Rubus glaucus) by-products: ultrasound-assisted extraction of total anthocyanins |
title_sort |
valorization of mulberry (rubus glaucus) by-products: ultrasound-assisted extraction of total anthocyanins |
description |
In this study, the objective was to establish parameters of optimization of the factors such as solvent concentration, extraction time and liquid-to-solid ratio in ultrasound-assisted extraction (UAE) of total anthocyanins from mulberry by-products. The study sample corresponds to mature fruits that did not comply with the size demanded by the market (by-product). Three independent variables including extraction time (6-74 min), liquid-solid ratio (33-66.16 mL/g), and ethanol concentration (63-96%) were investigated. A rotatable central composite design (CCD) and response surface methodology (RSM) was used to investigate the effect of process variables. The optimum conditions of ultrasound-assisted extraction obtained through response surface methodology were as follow: extraction time, 20 min; liquid to solid ratio, 60:1 mL/g, and ethanol concentration, 90%, allowed to obtain a maximum concentration of 259.66 mg/L. To validate the optimized model, the experimental values were compared with the predicted values to check the adequacy of the model. Ultrasound extraction was 13.60% higher than maceration technique and reduces the time from 24h to 20 minutes. The results show that ultrasonic-assisted extraction as a promising agro-industrial process in the recovery of anthocyanins from mulberry by-products. |
publisher |
Facultad de Ciencias Agrarias-UNCuyo |
publishDate |
2019 |
url |
https://revistas.uncu.edu.ar/ojs3/index.php/RFCA/article/view/2708 |
topic |
diseño compuesto central metodología de superficie de respuesta colorante natural optimización central composite design response surface methodology natural colorant optimization |
topic_facet |
diseño compuesto central metodología de superficie de respuesta colorante natural optimización central composite design response surface methodology natural colorant optimization |
work_keys_str_mv |
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